Prescott, Hillary A.: The Crystal Structures and Thermal Behavior of Hydrogen Monofluorophosphates and Basic Monofluorophosphates with Alkali Metal and N-containing Cations

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References

1 . K. D. Kreuer , "Proton Conductivity: Materials and Applications" . Chem. Mater. 8 (1996) 610 .

2 . A. I. Baranov, L. A. Shuvalov, N. M. Schagina , "Superion conductivity and phase transitions in CsHSO4 and CsHSeO4 crystals" . JETP Lett. 36 (1982 ) 459 .

3 . C. J. P. Grotthus , Ann. Chim. 58 (1806) 54 .

4 . K. D. Kreuer, A. Rabenau, W. Weppner , "Vehikel-Mechanismus, ein neues Modell zur Deutung der Leitfähigkeit schneller Protonenleiter" . Angew. Chem. 94 (1982 ) 224 .

5 . T. Muiri, A. Daoud, P. Gravereau , "Crystal structure and vibrational study of mixed rubidium-caesium hydrogen sulphate Cs0.1Rb0.9HSO4" . J. Alloys Compd. 205 (1994) 21 .

6 . K. Itoh, T. Ukeda, T. Ozaki, E. Nakamura , "Redetermination of the Structure of Caesium Hydrogensulfate" . Acta Crystallogr. C46 (1990) 358 .

7 . R. Pepinsky, K. Vedam, S. Hoshino, Y. Okaya , "Ammonium Hydrogen Sulfate: A New Ferroelectric with Low Coercive Field" . Phys. Rev. 111 (1958) 1508 .

8 . K. Itoh, H. Ohno, S. Kuragaki , "Disordered Structure of Ferroelectric Rubidium Hydrogen Sulfate in the Paraelectric Phase" . J. Phys. Soc. Jpn. 64 (1995) 479-84 .

9 . F. Payan, R. Haser , "On the Hydrogen Bonding in Potassium Hydrogen Sulphate. Comparison with a Previous Crystal Structure Determination" . Acta Crystallogr. B32 (1976 ) 1875-9 .

10 . E. Kemnitz, C. Werner, S. I. Troyanov , "Structural Chemistry of alkaline metal hydrogen sulfates. A review of new structural data. Part II. Hydrogen Bonding Systems" . Eur. J. Solid State Inorg. Chem. 33 (1996) 581-96 .

11 . A. Stiewe , "Strukturchemische Untersuchungen an sauren Oxosalzen" . Ph.D. Thesis : Humboldt University, Berlin, Germany , 2000 .

12 . C. Werner , "Strukturaufklärung von Hydrogensulfaten der Alkali- und Erdalkalimetalle" . Ph.D. Thesis : Humboldt University, Berlin, Germany , 2000 .

13 . N. Wiberg , Lehrbuch der Anorganische Chemie ; 101st ed., Walter de Gruyter : Berlin, Germany , 1995 ; p 133 .

14 . R. F. Weinland, J. Alfa , "Über ein Fluorsulfat und ein Fluorphosphat des Kaliums bzw. Rubidium" . Ber. Dtsch. Chem. Ges. B31 (1898) 123-6 .

15 . R. F. Weinland, J. Alfa , "Über fluorierte Phosphate, Sulfate, Selenate, Tellurate und Dithionate" . Z. Anorg. Chem. 21 (1899) 43 .

16 . W. Lange , "The Chemistry of the Fluoro Acids of Fourth, Fifth, and Sixth Group Elements" . In Fluorine Chemistry ; J. H. Simons, Ed.; Academic Press : New York , 1950 ; Vol. 1 , pp 140-9 .

17 . D. A. Palgrave , "Fluorophosphoric Acids and the Fluorophosphates" . In A comprehensive treatise on inorganic and theoretical chemistry ; J. W. Mellor, Ed.; Longmans, Green, and Co.: London , 1971 ; Vol. 8 (Suppl. 3) , pp 843-71 .

18 . W. Lange , "Über die Monofluorophosphorsäure und die Ähnlichkeiten ihrer Salze mit den Sulfaten" . Ber. Dtsch. Ges. Chem. B62 (1929) 793-801 .

19 . J. R. van Wazer, Ed. , Phosphorus and its Compounds; Interscience Publishers: New York, 1958 ; Vol. 1, pp 803-17.

20 . W. Granier, J. Durand, L. Cot , "Composés oxyfluorés du phosphore V" . Rev. Chim. Min. 12 (1975) 147-55 .

21 . K. Heide, D.-H. Menz, C. Schmidt, L. Kolditz , "Zur thermischen Zersetzung von CaPO3F.2H2O" . Z. Anorg. Allg. Chem. 520 (1985) 32-8 .

22 . V. Q. Kinh, G. Montel , "Sur la décomposition du monofluorophosphate de calcium et la formation du pyrophosphate de calcium alpha métastable" . Compt. rend. 249 (1959) 117-9 .

23 . D.-H. Menz, K. Heide, C. Kunert, C. Mensing, L. Kolditz , "Zur thermischen Zersetzung von SrPO3F.H2O" . Z. Anorg. Allg. Chem. 540/541 (1986 ) 191-7 .

24 . V. Q. Kinh, G. Montel , "Sur la transformation par chauffage du monofluorophosphate de strontium en fluoroapatite" . Compt. rend. 252 (1961) 3809-11 .

25 . D.-H. Menz, L. Kolditz , "Synthese und thermisches Verhalten von Mg(NH4)2(PO3F)2·2H2O" . Z. Chem. 25 (1985) 189-90 .

26 . J. Neels, H. Grunze , "Darstellung von Alkalihydrogenmonofluorophosphaten" . Z. Anorg. Allg. Chem. 360 (1968 ) 284-92 .

27 . J. Neels, H. Grunze , "Kondensationsvorgänge beim Erhitzen von Kaliumhydrogenmonofluorophosphat, K[HPO3F]" . Z. Chem. 18 (1978) 373 .

28 . A. K. Idrissi, M. Rafiq, P. Gougeon, R. Guerin , "Anilinium Hydrogen Monofluorophosphate, C6H8N+·HPO3F-" . Acta Crystallogr. C51 (1995) 1359-61 .

29 . N. N. Greenwood, A. Earnshaw , Chemistry of the Elements ; 1st ed., VCH Verlagsgesellschaft : Weinheim , 1990 ; p 63 . translated by K. Hückmann

30 . A. F. Wells , Structural Inorganic Chemistry ; 5th ed., Clarendon Press : Oxford , 1984 ; p 357 .

31 . P. Gilli, V. Bertolasi, V. Ferretti, G. Gilli , "Covalent Nature of the Strong Homonuclear Hydrogen Bond. Study of the O-H...O System by Crystal Structure Correlation Methods" . J. Am. Chem. Soc. 116 (1994) 909-15 .

32 . E. Kemnitz, S. I. Troyanov , "Hydrogen Bonding Systems in Acid Metal Sulfates and Selenates" . Advances in Molecular Structure Research ; M. Hargittai, I. Hargittai; Jai Press Inc. : London , 1998 ; Vol. 4 , pp 79-115 .

33 . I. P. Makarova, E. E. Rider, V. A. Sarin, I. P. Aleksandrova, V. I. Simonov , "Neutron structure studies of the ferroelectric and paraelectric phases of rubidium acid selenate" . Kristallografiya 34 (1989) 853-61 .

34 . J. Baran, T. Lis , "Structure of cesium hydrogen selenate" . Acta Crystallogr. C43 (1987) 811-3 .

35 . P. Dera, A. Katrusiak, M. Szafranski , "Structures of Diguanidinium Sulfate and Guanidinium Hydrogen Sulfate" . Pol. J. Chem. 74 (2000) 1637-44 .

36 . E. J. Sonneveld, J. W. Visser , "A New Modification of Sodium Hydrogensulphate" . Acta Crystallogr. B34 (1978) 643-5 .

37 . M. A. Zakharov, S. Troyanov, V. B. Rybakov, L. A. Aslanov, E. Kemnitz , Kristallografiya 44 (1999) 448 .

38 . N. G. Hainovsky, Yu. T. Pavlukhim, E. Hairetdinov , Solid State Ionics 20 (1986) 249 .

39 . F. A. Cotton, B. A. Frenz, D. L. Hunter , "The Structure of Potassium Hydrogen Sulfate" . Acta Crystallogr. B31 (1975) 302-5 .

40 . J. Baran, T. Lis , "Structure of potassium hydrogenselenate" . Acta Crystallogr. C42(3) (1986) 270-2 .

41 . C. Werner, S. Troyanov, E. Kemnitz, H. Worzala , "Hydrogen sulfate with disordered hydrogen atoms-synthesis and structure of Li[H(HSO4)2](H2SO4)2 and refinement of the structure of alpha-NaHSO4" . Z. Anorg. Allg. Chem. 622 (1996) 337-42 .

42 . D. B. Dell'Amico, F. Calderazzo, F. Marchetti, St. Merlino , Chem. Mater. 10 (1998) 524 .

43 . A. Stiewe, S. Troyanov, E. Kemnitz , "Synthesis and crystal structure of metal(I) hydrogen sulfates Ag(H3O)(HSO4)2, Ag2(HSO4)2(H2SO4), AgHSO4, and Hg2(HSO4)2" . Z. Anorg. Allg. Chem. 625 (1999) 329 .

44 . Y. Noda, S. Uchiyama, K. Kafuku, H. Kasatani, H. Terauchi , "Structure Analysis and Hydrogen Bond Character of K3(HSO4)2" . J. Phys. Soc. Jpn. 59 (1990) 2804-10 .

45 . M. Ichikawa, S. Sato, M. Komukae, T. Osaka , "Structure of Ferroelastic K3H(SeO4)2" . Acta Crystallogr. C48 (1992) 1569-71 .

46 . S. Fortier, M. E. Fraserm R. D. Heyding , "Structure of Trirubidium Hydrogenbis(sulfate), Rb3H(SO4)2" . Acta Crystallogr. C41 (1985) 1139-41 .

47 . I. P. Makarova, I. A. Verin, N. M. Shchagina , "Crystal structure of rubidium selenate (Rb3H(SeO4)2)" . Kristallografiya 31 (1986) 178-80 .

48 . R. Melzer, R. Sonntag, K. S. Knight , "Rb3H(SeO4)2 at 4K by Neutron Powder Diffraction" . Acta Crystallogr. C52 (1996) 1061-3 .

49 . M. Ichikawa, T. Gustafsson, I. Olovsson , "Structural Study of the low-temperature phase transition in tricesium deuterium diselenate" . Acta Crystallogr. B48 (1992) 633-9 .

50 . R. Sonntag, R. Melzer, K. S. Knight , "Determination of the hydrogen position in Cs3H(SeO4)2 at 483 K" . Physica B 234-236 (1997) 89-91 .

51 . W. Joswig, H. Fuess, G. Ferraris , "Neutron Diffraction Study of the Hydrogen Bond in Trisodium Hydrogenbissulphate and a Survey of Very Short O-H...O Bonds" . Acta Crystallogr. B38 (1982) 2798-2801 .

52 . S. Suzuki, A. Makita , "The Crystal Structure of Triammonium Hydrogen Disulphate, (NH4)3H(SO4)2" . Acta Crystallogr. B34 (1978) 732-5 .

53 . N. A. Tikhomirova, L. A. Shuvalov, L. I. Dontsova, L. G. Bulatova, L. Z. Potikha , "Dynamics of domain structure in collinear ferroelectric crystals TGs and GASH" . Kristallografiya 31(6) (1986) 1152-9 .

54 . R. F. Baggio, M. A. R. De Benyacar, B. O. Perazzo, P. K. De Perazzo , "Crystal Structure of ferroelectric guanidinium uranyl sulfate trihydrate" . Acta Crystallogr. B33 (1977) 3495-9 .

55 . Römpp Lexikon Chemie, Version 2.0 [CD-ROM]; Georg-Thieme Verlag : Stuttgart/New York , 1999 .

56 . F. Seel, E. Steigner, I. Burger , "Determination of fluorine" . Angew. Chem. 76(12) (1964) 532-4 .

57 . W. Herrendorf , "Ph. D. Thesis, University of Karlsruhe, Karlsruhe, Germany" . Intergrated in X-Shape Program: Crystal Optimization for Numerical Absorption Correction ; Revision 1.01, (Stoe & Cie GmbH Deutschland) : Darmstadt , 1996 .

58 . G. M. Sheldrick , SHELXS-86: Program for Crystal Structure Determination ; University of Göttingen, Göttingen, Germany , 1990 .

59 . G. M. Sheldrick , SHELXS-97: Program for Crystal Structure Determination ; University of Göttingen, Göttingen, Germany , 1990 .

60 . G. M. Sheldrick , SHELXL-93: Program for the Refinement of Crystal Structures ; University of Göttingen, Göttingen, Germany , 1993 .

61 . G. M. Sheldrick , SHELXL-97: Program for the Refinement of Crystal Structures ; University of Göttingen, Göttingen, Germany , 1997 .

62 . N. E. Brese, M. O'Keefe , "Bond-Valence Parameters for Solids" . Acta Crystallogr. B47 (1991) 192 .

63 . I. D. Brown , "Chemical and Steric Constraints in Inorganic Solids" . Acta Crystallogr. B48 (1992 ) 553-72 .

64 . L. Pauling , "The principles determining the structure of complex ionic crystals" . J. Am. Chem. Soc. 51 (1929) 1010-26 .

65 . PCPDFWIN , Version 1.30 [CD-ROM], International Centre of Diffraction Data : Newtown Square, Pennsylvania, USA , 1997 .

66 . J. O. Hill , For Better Thermal Analysis III, Special Edition of the International Confederation for Thermal Analysis (ICTA) ; 1991 .

67 . K. Heide , Dynamische Thermische Analysenmethoden ; VEB Deutscher Verlag für Grundstoffindustrie : Leipzig , 1982 .

68 . H. K. Cammenga, W. Eysel, E. Gmelin, W. Hemminger, G. W. H. Höhne, S. M. Sarge , "The temperature calibration of scanning calorimeters. Part 2. Calibraiton substances" . Thermochim. Acta 219 (1993) 333-42 .

69 . W. Hemminger, H. K. Cammenga , Methoden der Thermischen Analyse ; Springer-Verlag Berlin : Heidelberg , 1989 .

70 . U. Schülke, R. Kayser , "Herstellung von Fluorophosphaten, Difluorophosphaten, Fluorophosphaten und Fluorophosphiten in fluoridhaltigen Harnstoffschmelzen" . Z. Anorg. Allg. Chem. 600 (1991) 221-6 .

71 . PDF-No. 21-1120 , Ref. 26 .

72 . PDF-No. 18-1215 , Ref. Ferguson, Nielsen, Monsanto Research Corporation, Dayton, Ohio, USA ; Private Communication, 1963 .

73 . A. Perloff , "The Crystal Structures of Hydrated Calcium and Ammonium Monofluorophosphates: CaPO3F·2H2O and (NH4)2PO3F·H2O" . Acta Crystallogr. C53 (1997) 2183-91 .

74 . N. Ohama, M. Machida, Y. Kunifuji , "Structure of tetramethylammonium dihydrogen orthophosphate monohydrate" . Acta Crystallogr. C43 (1987) 962-4 .

75 . A. Waskowska , "Diguanidinium hexafluorosilicate" . Acta Crystallogr. C53 (1997) 128-30 .

76 . W. Lange , "Method of Production of Anhydrous Monofluorophosphoric Acid" . U. S. Patent 2,408,785 , Oct. 8, 1946 .

77 . H. A. Prescott, S. I. Troyanov, E. Kemnitz , "Two Modification of NH4HPO3F: Synthesis and Crystal Structure" . Z. Anorg. Allg. Chem. 629 (2002) in press .

78 . H. A. Prescott, S. I. Troyanov, E. Kemnitz , "The crystal structures of two hydrogen monofluorophosphates: CsHPO3F and Cs3(NH4)2(HPO3F)3(PO3F)2" . Z. Kristallogr. 215 (2000) 240-5 .

79 . PDF-No. 21-0374; Ref. 26 .

80 . PDF-No. 21-0987; Ref. 26 .

81 . H. A. Prescott, S. I. Troyanov, E. Kemnitz , "The Synthesis and Crystal Structures of Two New Hydrated Sodium Monofluorophosphates: NaHPO3F·2.5H2O (I) and Na2PO3F·10H2O (II) " . J. Solid State Chem. 156 (2001) 415-21 .

82 . A. R. West , Grundlage der Festkörperchemie ; VCH Verlaggesellschaft : Weinheim , 1992 ; translated by M. Hartweg und U. Hartweg

83 . G. Liptay , Atlas of Thermoanalytical Curves ; Akadémiai Kiadó : Budapest , 1975 ; Vol. 4 , No. 205 .

84 . J. E. Macintyre, F. M. Daniel, V. M. Stirling, Eds. , Dictionary of Inorganic Compounds ; Chapman & Hall : London , 1992 .

85 . D. E. C. Corbridge , Phosphorus: An Outline of its Chemistry, Biochemistry, and Technology ; 4th ed., Elsevier : Oxford , 1990 ; p 231 .

86 . H. Falius , "Darstellung von Dikalium-difluorodiphosphat durch thermische Reaktion von Tetraphosphatdekaoxid mit Kaliumfluorid" . Angew. Chem. 80 (1968) 616 .

87 . P.A. Bernstein, F. A. Hohurst, M. Eisenberg, D. D. DesMarteau , "Preparation of Pure Difluorophosphoric Acid and mu-Oxo-bis(phosphoryl difluoride)" . Inorg. Chem. 10(7) (1971) 1549-51 .

88 . W. E. Hill, D. W. A. Sharp, C. B. Colburn , "NMR Spectra of Pyrophosphoryl Tetrafluoride and mu-Oxobis(thiophosphoryl Difluoride)" . J. Chem. Phys. 50(2) (1960) 612-5 .

89 . PDF-No. 11-648, Ref: P. de Wolff, Technische-Physische Dienst, Delft, The Netherlands , ICDD Grant-in-Aid .

90 . H. M. Ondik , "The structures of anhydrous sodium trimetaphosphate, Na3O9, and the monohydrate, Na3P3O9·H2O" . Acta Crystallogr. 18 (1965) 226-32 .

91 . H. A. Prescott, M. Feist, J. Przezdziak, E. Kemnitz , "The Thermal Behavior of NaHPO3F.2.5H2O" . Abstracts of Papers ; 2001 , 13th European Symposium on Fluorine Chemistry, Bordeaux, France , 1-P93 .

92 . C. C. Addison, J. W. Bailey, S. H. Bruce, M. F. A. Dove, R. C. Hibbert, N. Logan , "Chemistry in Fuming Nitric Acids-I. NMR Spectroscopic Study of PF5, HPO2F2, and P4O10 in the Solvent System 44 wt.% N2O4 in 100% HNO3" . Polyhedron 2 (1983) 651-6 .

93 . PDF-No. 11-650, Ref: P. de Wolff, Technische-Physische Dient. Delft, The Netherlands , ICDD Grant-in-Aid .

94 . P. D. Ray , "Isomorphism and chemical homology" . Nature 126 (1930) 310-11 .

95 . H. C: Goswani , "On the Study of some Monofluorophosphates and their Analogy and Isomorphism with Sulphates" . J. Indian Chem. Soc. 14 (1937) 660 .

96 . J. P. Ashmore, H. E. Petch , "The Structure of RbHSO4 in its Paraelectric Phase" . Can. J. Phys. 53 (1975) 2694-702 .

97 . R. Pepinsky, K. Vedam , "Ferroelectric transition in RbHSO4" . Phys. Rev. 117 (1960) 1502 .

98 . T. Asahi, K. Hasebe , "Crystal structure of the high pressure phase of RbHSO4" . J. Phys. Soc. Jpn. 65 (1996) 3233 .

99 . V. Varma, N. Ragavittal, C. N. R. Rao , "A Study of Superionic CsHSO4 and Cs1-xLixHSO4 by Vibrational Spectroscopy and X-ray Diffraction" . J. Solid State Chem. 106 (1993) 164-73 .

100 . R. J. Nelmes , "An X-ray Diffraction Determination of the Crystal Structure of Ammonium Hydrogen Sulphate above the Ferroelectric Transition" . Acta Crystallogr. B27 (1971 ) 272-81 .

101 . S. I. Troyanov, I. V. Morozov, M. Reehius, E. Kemnitz , "Synthesis of Two Modifications of (NH4)2SeO4(H3PO4) and Their Crystal Structure as Probed by X-ray and Neutron Diffraction" . Russ. J. Inorg. Chem. 44 (1999) 1924 .

102 . M. Catti, G. Ferraris, M. Franchini-Angela , "Hydrogen bonding in the crystalline state. NaHSO4·H2O (Matteuccite), a pseudosymmetric crystal structure" . Atti Accad. Sci. Torino, Cl. Fis., Mat. Nat. 109 (1975) 531-45 .

103 . S. I. Troyanov , Humboldt University, Berlin, Germany , Private Communication, 2001 .

104 . H. W. Ruben, D. H. Templeton, R. D. Rosenstein, I. Olovsson , "Crystal structure and entropy of sodium sulfate decahydrate" . J. Am. Chem. Soc. 83 (1961) 820-4 .

105 . H. A. Levy, G. C. Lisensky , "Crystal structures of sodium sulfate decahydrate (Glauber's salt) and sodium tetraborate decahydrate (borax). Redetermination by neutron diffraction" . Acta Crystallogr B34 (1978) 3502-10 .

106 . G. Brodale, W. F. Giauque , "Heat of hydration of sodium sulfate. Low-temperature heat capacity and entropy of sodium sulfate decahydrate" . J. Am. Chem. Soc. 80 (1958) 2042-4 .

107 . Structural Information has been deposited at the Fachinformationszentrum Karlsruhe, D-76344 Eggenstein-Leopoldshafen, Germany under the depository number : CSD-No. 411348 .

108 . M. Zeibig, B. Wallis, F. Möwius, M. Meisel , "Darstellung und Kristallstruktur von Kupfer(II)-monofluorophosphat-Dihydrat CuPO3F·2H2O" . Z. Anorg. Allg. Chem. 600 (1991) 231 .

109 . J. Durand, A. Larbot, L. Cot, M. Duprat, F. Dabosi , "Etude Structurale de ZnPO3F·2.5H2O Nouvel Inhibteur de Corrosion" . Z. Anorg. Allg. Chem. 504 (1983) 163-72 .

110 . M. Berraho, C. K'Rha, A. Vegas, M. Rafiq , "Structure of Ni(H2O)6(NH4)2(PO3F)2" . Acta Crystallogr. C48 (1992) 1350-52 .

111 . R. D. Shannon, C. T. Prewitt , "Effective ionic radii in oxides and fluorides" . Acta Crystallogr. B25 (1969 ) 925-46 .

112 . R. D. Shannon, C. T. Prewitt , Acta Crystallogr. A32 (1976) 751 .

113 . J. Duran, W. Garnier, L. Cot, J. L. Galigné , "Etudes Structurales de Composés Oxyfluorés du P(V).III. Structure Cristallin de NaK3(PO3F)2" . Acta Crystallogr. B31 (1975) 1533-5 .

114 . G. Rother , "Synthese, Struktur und thermisches Verhalten von Fluorometallaten(III) mit organischen N-haltigen Kationen" . Ph.D. Thesis : Humboldt University, Berlin, Germany , 1998 .

115 . A. Vij, X. Zhang, K. O. Christe , "Crystal structure of F2NO+AsF6- and method for extracting meaningful geometries from oxygen/fluorine disordered crystal structures" . Inorg. Chem. 40 (2001) 416 .

116 . E. C. Kostanek, W. R. Busing , "A Single-Crystal Neutron-Diffraction Study of Urea-Phosphoric Acid" . Acta Crystallogr. B28 (1972) 2454 .


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