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2020-04-09Zeitschriftenartikel DOI: 10.3390/nano10040713
Advances in Nickel Nanoparticle Synthesis via Oleylamine Route
Heilmann, Maria cc
Kulla, Hannes
Prinz, Carsten
Bienert, Ralf cc
Reinholz, Uwe
Guilherme Buzanich, Ana cc
Emmerling, Franziska cc
Mathematisch-Naturwissenschaftliche Fakultät
Nickel nanoparticles are an active research area due to their multiple applications as catalystsin different processes. A variety of preparation techniques have been reported for the synthesisof these nanoparticles, including solvothermal, microwave-assisted, and emulsion techniques.The well-studied solvothermal oleylamine synthesis route comes with the drawback of needingstandard air-free techniques and often space-consuming glassware. Here, we present a facile andstraightforward synthesis method for size-controlled highly monodisperse nickel nanoparticlesavoiding the use of, e.g., Schlenk techniques and space-consuming labware. The nanoparticlesproduced by this novel synthetic route were investigated using small-angle X-ray scattering,transmission electron microscopy, X-ray diffraction, and X-ray spectroscopy. The nanoparticles werein a size range of 4–16 nm, show high sphericity, no oxidation, and no agglomeration after synthesis.
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DOI
10.3390/nano10040713
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https://doi.org/10.3390/nano10040713
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<a href="https://doi.org/10.3390/nano10040713">https://doi.org/10.3390/nano10040713</a>