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2020-04-09Zeitschriftenartikel DOI: 10.3390/nano10040713
Advances in Nickel Nanoparticle Synthesis via Oleylamine Route
dc.contributor.authorHeilmann, Maria
dc.contributor.authorKulla, Hannes
dc.contributor.authorPrinz, Carsten
dc.contributor.authorBienert, Ralf
dc.contributor.authorReinholz, Uwe
dc.contributor.authorGuilherme Buzanich, Ana
dc.contributor.authorEmmerling, Franziska
dc.date.accessioned2021-02-18T08:29:02Z
dc.date.available2021-02-18T08:29:02Z
dc.date.issued2020-04-09none
dc.date.updated2020-05-05T20:46:08Z
dc.identifier.urihttp://edoc.hu-berlin.de/18452/23110
dc.description.abstractNickel nanoparticles are an active research area due to their multiple applications as catalystsin different processes. A variety of preparation techniques have been reported for the synthesisof these nanoparticles, including solvothermal, microwave-assisted, and emulsion techniques.The well-studied solvothermal oleylamine synthesis route comes with the drawback of needingstandard air-free techniques and often space-consuming glassware. Here, we present a facile andstraightforward synthesis method for size-controlled highly monodisperse nickel nanoparticlesavoiding the use of, e.g., Schlenk techniques and space-consuming labware. The nanoparticlesproduced by this novel synthetic route were investigated using small-angle X-ray scattering,transmission electron microscopy, X-ray diffraction, and X-ray spectroscopy. The nanoparticles werein a size range of 4–16 nm, show high sphericity, no oxidation, and no agglomeration after synthesis.eng
dc.language.isoengnone
dc.publisherHumboldt-Universität zu Berlin
dc.rights(CC BY 4.0) Attribution 4.0 Internationalger
dc.rights.urihttps://creativecommons.org/licenses/by/4.0/
dc.subjectnanoparticle synthesiseng
dc.subjectnickel nanoparticleseng
dc.subjectSAXSeng
dc.subjectTEMeng
dc.subjectXASeng
dc.subject.ddc540 Chemie und zugeordnete Wissenschaftennone
dc.titleAdvances in Nickel Nanoparticle Synthesis via Oleylamine Routenone
dc.typearticle
dc.identifier.urnurn:nbn:de:kobv:11-110-18452/23110-7
dc.identifier.doi10.3390/nano10040713none
dc.identifier.doihttp://dx.doi.org/10.18452/22498
dc.type.versionpublishedVersionnone
local.edoc.container-titleNanomaterialsnone
local.edoc.pages13none
local.edoc.type-nameZeitschriftenartikel
local.edoc.institutionMathematisch-Naturwissenschaftliche Fakultätnone
local.edoc.container-typeperiodical
local.edoc.container-type-nameZeitschrift
local.edoc.container-publisher-nameMDPInone
local.edoc.container-publisher-placeBaselnone
local.edoc.container-volume10none
local.edoc.container-issue4none
dc.description.versionPeer Reviewednone
local.edoc.container-articlenumber713none
dc.identifier.eissn2079-4991
local.edoc.affiliationHeilmann, Maria; BAM Bundesanstalt für Materialforschung und -prüfung, Richard-Willstätter Strasse 11, D-12489 Berlin, Germany, maria.heilmann@bam.de Humboldt-Universität zu Berlin, Department of Chemistry, Brook-Taylor Strasse 2, D-12489 Berlin, Germany, maria.heilmann@bam.de; Humboldt-Universität zu Berlin, Department of Chemistry, Brook-Taylor Strasse 2, D-12489 Berlin, Germanynone
local.edoc.affiliationKulla, Hannes; BAM Bundesanstalt für Materialforschung und -prüfung, Richard-Willstätter Strasse 11, D-12489 Berlin, Germany, hkulla11@gmail.comnone
local.edoc.affiliationPrinz, Carsten; BAM Bundesanstalt für Materialforschung und -prüfung, Richard-Willstätter Strasse 11, D-12489 Berlin, Germany, Carsten.Prinz@bam.denone
local.edoc.affiliationBienert, Ralf; BAM Bundesanstalt für Materialforschung und -prüfung, Richard-Willstätter Strasse 11, D-12489 Berlin, Germany, Ralf.Bienert@bam.denone
local.edoc.affiliationReinholz, Uwe; BAM Bundesanstalt für Materialforschung und -prüfung, Richard-Willstätter Strasse 11, D-12489 Berlin, Germany, Uwe.Reinholz@bam.denone
local.edoc.affiliationGuilherme Buzanich, Ana; BAM Bundesanstalt für Materialforschung und -prüfung, Richard-Willstätter Strasse 11, D-12489 Berlin, Germany, Ana.Buzanich@bam.denone
local.edoc.affiliationEmmerling, Franziska; BAM Bundesanstalt für Materialforschung und -prüfung, Richard-Willstätter Strasse 11, D-12489 Berlin, Germany, franziska.emmerling@bam.de Humboldt-Universität zu Berlin, Department of Chemistry, Brook-Taylor Strasse 2, D-12489 Berlin, Germany, franziska.emmerling@bam.de; Humboldt-Universität zu Berlin, Department of Chemistry, Brook-Taylor Strasse 2, D-12489 Berlin, Germanynone

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