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2022-03-19Zeitschriftenartikel DOI: 10.1002/cctc.202200029
Chlorodefluorination of Fluoromethanes and Fluoroolefins at a Lewis Acidic Aluminum Fluoride
Pan, Xinzi cc
Talavera, Maria cc
Scholz, Gudrun cc
Braun, Thomas cc
Mathematisch-Naturwissenschaftliche Fakultät
Chlorodefluorination reactions of fluoromethanes and fluoroolefins catalysed by the highly Lewis acidic nanoscopic aluminum chlorofluoride (ACF, AlClxF3−x, x≈0.05–0.3) in the presence of ClSiEt3 were studied. Both fluoromethanes and fluoroolefins convert under mild reaction conditions by fluorine-chlorine exchange steps into chlorinated fluoro derivatives. MAS NMR studies provided information on the interaction of silanes and hexafluoropropene with the ACF surface.
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(CC BY-NC-ND 4.0) Attribution-NonCommercial-NoDerivatives 4.0 International(CC BY-NC-ND 4.0) Attribution-NonCommercial-NoDerivatives 4.0 International(CC BY-NC-ND 4.0) Attribution-NonCommercial-NoDerivatives 4.0 International(CC BY-NC-ND 4.0) Attribution-NonCommercial-NoDerivatives 4.0 International
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DOI
10.1002/cctc.202200029
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https://doi.org/10.1002/cctc.202200029
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<a href="https://doi.org/10.1002/cctc.202200029">https://doi.org/10.1002/cctc.202200029</a>